N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester

Base Information

• Chemical Name: N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester
• CAS No.: 1160060-28-5
• Molecular Formula: C₂₈H₃₁N₃O₃
• Molecular Weight: 457.572
• Mol file: 1160060-28-5.mol

Synonyms:N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester

Chemical Property of N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester

There total 1 articles about N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

L-valine ethyl ester (17431-03-7) + 9-(3-phenylpropyl)-β-carboline-3-carboxylic acid → N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester (1160060-28-5)

Guidance literature:

9-(3-phenylpropyl)-β-carboline-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃;

L-valine ethyl ester; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.ejmech.2009.12.060

Reference yield: 96.0%

N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester (1160060-28-5) → N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine (1223075-71-5)

Guidance literature:

N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester; With sodium hydroxide; In ethanol; water; for 1h; Reflux;

With hydrogenchloride; In water;

DOI:10.1016/j.ejmech.2009.12.060

Reference yield: 40.0%

N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine ethyl ester (1160060-28-5) + benzyl bromide (100-39-0) → Br(1-)*C35H38N3O3(1+) (1223075-81-7)

Guidance literature:

In ethyl acetate; Reflux;

DOI:10.1016/j.ejmech.2009.12.060

upstream raw materials:

L-valine ethyl ester

Downstream raw materials:

N-(9-(3-phenylpropyl)-beta-carboline-3-carbonyl)-L-valine

Br^(1-)*C₃₅H₃₈N₃O₃⁽¹⁺⁾