N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

Base Information

Chemical Name:N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)
CAS No.:1607026-79-8
Molecular Formula:C₃₄H₂₆Cl₂N₆O₄S₂
Molecular Weight:717.656
Hs Code.:

Synonyms:N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

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Chemical Property of N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

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Technology Process of N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

There total 5 articles about N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₁₄H₉ClN₂O₂S

: 95-54-5
1,2-diamino-benzene

: 1607026-79-8
N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

Guidance literature:: In acetonitrile; at 60 - 70 ℃; for 3h;
DOI:10.2174/15701808113109990045

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1607026-79-8
N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid

2: potassium carbonate / acetonitrile

3: sodium hydroxide; water / methanol

4: acetonitrile

5: acetonitrile / 3 h / 60 - 70 °C

With sulfuric acid; water; potassium carbonate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.2174/15701808113109990045

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 1607026-79-8
N,N'-(1,2-phenylenebis(azanediyl))bis(thioxomethylene)bis(2-((6-chloropyridin-3-yl)methoxy)benzamide)

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile

2: sodium hydroxide; water / methanol

3: acetonitrile

4: acetonitrile / 3 h / 60 - 70 °C

With water; potassium carbonate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.2174/15701808113109990045