potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

Base Information

Chemical Name:potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)
CAS No.:125878-73-1
Molecular Formula:C₁₆H₂₆BOSi*K
Molecular Weight:312.377
Hs Code.:

Synonyms:potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

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Technology Process of potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

There total 1 articles about potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 125212-51-3
(E)-2-diethylboryl-1-phenyl-1-trimethylsilyl-1-butene

: 125878-73-1
potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; byproducts: CH4; dropwise addn. of the cis-2-boryl-1-silylalkene to a suspn. of anhyd. KOH (within 1 h), temp. rise to about 40°C under CH4 cleavage, heating under reflux (2 h), removing of solvent (14 torr); drying (0.001 torr); elem. anal.;

Reference yield: 94.0%

: 1529-47-1
chlorotrimethylgermane

: 125878-73-1
potassium (4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1,2,5-oxasilaboratolate)

: 132126-12-6
4,5,5-triethyl-2,5-dihydro-2,2-dimethyl-3-phenyl-1-(trimethylgermyl)-1,2,5-oxoniasilaboratole

Guidance literature:: In diethyl ether; byproducts: KCl; (Ar); added dropwise a soln. of Ge-compound to soln. of B-compound; refluxed for 4 h; filtered; evapd. (vac.); elem. anal.;