N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

Base Information

Chemical Name:N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide
CAS No.:1197160-67-0
Molecular Formula:C₂₉H₃₇N₉O₄
Molecular Weight:575.671
Hs Code.:

Synonyms:N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

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Chemical Property of N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

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Technology Process of N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

There total 2 articles about N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1197160-66-9
4-(3-(4-(4,6-bismorpholine-1,3,5-triazin-2-yl)phenyl)ureido)benzoic acid

: 108-00-9
N,N-dimethylethylenediamine

: 1197160-67-0
N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

Guidance literature:: 4-(3-(4-(4,6-bismorpholine-1,3,5-triazin-2-yl)phenyl)ureido)benzoic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;

N,N-dimethylethylenediamine; In 1-methyl-pyrrolidin-2-one;

Reference yield:

: 1197160-55-6
methyl 4-({[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}amino)benzoate

: 1197160-67-0
N-[2-(dimethylamino)ethyl]-4-{[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]carbamoyl}aminobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 8 h / Reflux

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

With lithium hydroxide monohydrate; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol;