methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate

Base Information

• Chemical Name: methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate
• CAS No.: 156558-06-4
• Molecular Formula: C₂₅H₃₁FO₃
• Molecular Weight: 398.518

Synonyms:methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate

Chemical Property of methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate

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Technology Process of methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate

There total 5 articles about methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

5-hydroxy-6,7-dimethylindan (28567-19-3) + methyl (S)-7-(4-fluorophenyl)-7-hydroxyheptanoate (156558-16-6) → methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate (156558-06-4) + C20H29FN2O6

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In diethyl ether; at 25 ℃; for 1h;

DOI:10.1039/p19960001021

Reference yield: 28.0%

5-hydroxy-6,7-dimethylindan (28567-19-3) + methyl (S)-7-(4-fluorophenyl)-7-hydroxyheptanoate (156558-16-6) → methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate (156558-06-4)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In toluene; at 10 ℃; for 1h;

DOI:10.1248/cpb.44.749

Reference yield: 9.0%

methyl (S)-7-(4-fluorophenyl)-7-hydroxyheptanoate (156558-16-6) + diethylazodicarboxylate (1972-28-7,218603-74-8) → methyl (R)-7-(5-hydroxy-6,7-dimethylindan-4-yl)-7-(4-fluorophenyl)heptanoate (156558-06-4) + C20H29FN2O6

Guidance literature:

With 5-hydroxy-6,7-dimethylindan; triphenylphosphine; In diethyl ether; at 25 ℃; for 1h;

DOI:10.1039/p19960001021

upstream raw materials:

5-hydroxy-6,7-dimethylindan

methyl (S)-7-(4-fluorophenyl)-7-hydroxyheptanoate

diethylazodicarboxylate

Downstream raw materials:

methyl (R)-7-(4-fluorophenyl)-7-(5-hydroxy-6,7-dimethyl-l-oxoindan-4-yl)heptanoate

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