((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

Base Information

Chemical Name:((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide
CAS No.:1012342-68-5
Molecular Formula:C₂₃H₁₈Cl₂N₂OP*I
Molecular Weight:567.193
Hs Code.:

Synonyms:((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

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Chemical Property of ((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

Chemical Property:

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Technology Process of ((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

There total 1 articles about ((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 603-35-0
triphenylphosphine

: 51356-03-7
4,5-dichloro-2-chloromethyl-pyridazin-3(2H)-one

: 1012342-68-5
((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

Guidance literature:: 4,5-dichloro-2-chloromethyl-pyridazin-3(2H)-one; With sodium iodide; In acetonitrile; for 10h; Heating;

triphenylphosphine; In acetonitrile; for 6h; Further stages.; Heating;
DOI:10.1002/jhet.5570450126

Reference yield: 67.0%

: 1012342-68-5
((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

: 100-52-7
benzaldehyde

: trans-4,5-dichloro-2-styrylpyridazine-3(2H)-one

Guidance literature:: With potassium tert-butylate; In acetonitrile; for 2h; Heating;
DOI:10.1002/jhet.5570450126

Reference yield:

: 1012342-68-5
((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide

: 4460-86-0,14374-62-0
asaraldehyde

: C₁₅H₁₄Cl₂N₂O₄

: 1185763-63-6
(E)-4,5-dichloro-2-(2,4,5-trimethoxystyryl)pyridazine-3(2H)-one

Guidance literature:: ((4,5-dichloro-6-oxopyridazine-1(6H)-yl)methyl)triphenyl phosphonium iodide; asaraldehyde; In acetonitrile; at 0 - 10 ℃; for 0.5h;

With potassium tert-butylate; In acetonitrile; for 2h;
DOI:10.1002/jhet.137