(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

Base Information

Chemical Name:(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine
CAS No.:753487-55-7
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:

Synonyms:(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

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Chemical Property of (2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

Chemical Property:

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Technology Process of (2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

There total 18 articles about (2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1009093-06-4
(2R,3R)-N-Boc-3-methoxy-phenylalaninol

: 753487-55-7
(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

Guidance literature:: With sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In aq. phosphate buffer; acetonitrile; at 20 ℃; for 16h; pH=6.4;
DOI:10.1021/acs.orglett.5b03292

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 874894-76-5
(2S,3R)-2-amino-3-methoxy-3-phenylpropanoic acid

: 753487-55-7
(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

Guidance literature:: With sodium hydroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 6h;
DOI:10.1021/ol049065n

Reference yield:

: 1009093-09-7
(2R,3R)-N-Boc-3-methoxy-1-O-(tert-butyldimethylsilyl)-phenylalaninol

: 753487-55-7
(2S,3R)-N-(tert-butyloxycarbonyl)-3-methoxyphenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chlorite / aq. phosphate buffer; acetonitrile / 16 h / 20 °C / pH 6.4

With sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; In tetrahydrofuran; aq. phosphate buffer; acetonitrile;
DOI:10.1021/acs.orglett.5b03292