N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide

Base Information

• Chemical Name: N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide
• CAS No.: 496945-42-7
• Molecular Formula: C₂₇H₃₅N₃O₄S
• Molecular Weight: 497.659

Synonyms:N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide

Chemical Property of N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide

Chemical Property:

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Technology Process of N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide

There total 1 articles about N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-(2-formylethyl)benzylcarbamate (496945-41-6) + N-(2-aminoethyl)naphthalene-2-sulfonamide (121494-42-6) → N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide (496945-42-7)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid;

DOI:10.1016/j.bmcl.2006.02.064

Reference yield:

N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide (496945-42-7) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]-N-methylamino]ethyl]-2-naphthalenesulfonamide

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid;

DOI:10.1016/j.bmcl.2006.02.064

Reference yield:

N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]amino]ethyl]-2-naphthalenesulfonamide (496945-42-7) + acetyl chloride (75-36-5) → N-[2-[N-acetyl-N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]-N-ethylamino]ethyl]-2-naphthalenesulfonamide (496945-65-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.166667h;

upstream raw materials:

tert-butyl 4-(2-formylethyl)benzylcarbamate

N-(2-aminoethyl)naphthalene-2-sulfonamide

Downstream raw materials:

N-[2-[N-acetyl-N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]-N-ethylamino]ethyl]-2-naphthalenesulfonamide

N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propyl]-N-ethylamino]ethyl]-2-naphthalenesulfonamide

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