tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Base Information

Chemical Name:tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate
CAS No.:1237518-83-0
Molecular Formula:C₃₂H₃₆N₂O₆
Molecular Weight:544.648
Hs Code.:

Synonyms:tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

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Chemical Property of tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

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Technology Process of tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

There total 9 articles about tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237518-21-6
tert-butyl 2-amino-4-(2-methoxyphenyl)benzoate

: C₁₄H₁₆ClNO₃

: 1237518-83-0
tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 1237518-05-6
2-acetoxy-5-(piperidin-1-yl)benzoic acid

: 1237518-83-0
tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C / Cooling with ice

2: pyridine / dichloromethane / 1.5 h / 20 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 5720-06-9
2-Methoxyphenylboronic acid

: 1237518-83-0
tert-butyl 2-(2-acetoxy-5-(piperidin-1-yl)benzamido)-4-(2-methoxyphenyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 2.5 h / Reflux; Inert atmosphere

2: sodium formate; acetic acid / palladium 10% on activated carbon / isopropyl alcohol; water / 2 h / Reflux

3: pyridine / dichloromethane / 1.5 h / 20 °C

With pyridine; sodium formate; sodium carbonate; acetic acid; bis-triphenylphosphine-palladium(II) chloride; palladium 10% on activated carbon; In 1,2-dimethoxyethane; dichloromethane; water; isopropyl alcohol;