C₂₇H₃₇NO₃

Base Information

• Chemical Name: C₂₇H₃₇NO₃
• CAS No.: 1378032-36-0
• Molecular Formula: C₂₇H₃₇NO₃
• Molecular Weight: 423.596
• Mol file: 1378032-36-0.mol

Synonyms:C₂₇H₃₇NO₃

Chemical Property of C₂₇H₃₇NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₇NO₃

There total 5 articles about C₂₇H₃₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) + 1-Benzyloxy-2-methoxy-4-(3-nitro-propyl)-benzene (127766-48-7) → C27H37NO3 (1378032-36-0)

Guidance literature:

With dmap; acetic anhydride; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.03.092

Reference yield:

4-allyl-1-benzyloxy-2-methoxybenzene (57371-42-3) → C27H37NO3 (1378032-36-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 3 h / 20 °C

1.2: 3 h / 0 °C

2.1: silver nitrate; sodium nitrite / water / 10 h / 20 °C / Darkness

3.1: dmap; acetic anhydride / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; iodine; acetic anhydride; silver nitrate; sodium nitrite; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/j.tetlet.2012.03.092

Reference yield:

4-allylguaiacol (97-53-0) → C27H37NO3 (1378032-36-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 4 h / 20 °C

2.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 3 h / 20 °C

2.2: 3 h / 0 °C

3.1: silver nitrate; sodium nitrite / water / 10 h / 20 °C / Darkness

4.1: dmap; acetic anhydride / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; iodine; acetic anhydride; potassium carbonate; silver nitrate; sodium nitrite; In tetrahydrofuran; dichloromethane; water; acetonitrile;

DOI:10.1016/j.tetlet.2012.03.092

upstream raw materials:

4-allylguaiacol

1-Decene

1-Benzyloxy-2-methoxy-4-(3-nitro-propyl)-benzene

4-allyl-1-benzyloxy-2-methoxybenzene

Downstream raw materials:

C₂₇H₃₈O₄

5-hydroxy-1-(4-hydroxy-3-methoxyphenyl)tridecan-3-one