7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Base Information

Chemical Name:7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate
CAS No.:642478-73-7
Molecular Formula:C₃₉H₃₁N₄O₉P
Molecular Weight:730.67
Hs Code.:

Synonyms:7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Suppliers and Price of 7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

There total 5 articles about 7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1623-08-1
phosphoric acid dibenzyl ester

: 642478-70-4
7-N-acetyldemethyllavendamycin β-hydroxyethyl ester

: 642478-73-7
7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 4 - 4.2h; Product distribution / selectivity;

Reference yield:

: N-(benzyloxycarbonyl)tryptophan β-hydroxyethyl ester

: 642478-73-7
7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / HCOONH₄ / Pd/C / dimethylformamide / 4.5 h / 20 °C

2: 94 percent / methoxybenzene; dimethylformamide / 5.5 h / 95 - 160 °C

3: 142 mg / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

With ammonium formate; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methoxybenzene; N,N-dimethyl-formamide; 2: Pictet-Spengler condensation / 3: Mitsunobu reaction;
DOI:10.1021/jm0304414

Reference yield:

: 13058-16-7
N-[(phenylmethoxy)carbonyl]-DL-tryptophan

: 642478-73-7
7-N-acetyldemethyllavendamycin β-hydroxyethyl ester dibenzyl phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / Et₃N / dibutyl ether / 5 h / Heating

2: 87 percent / HCOONH₄ / Pd/C / dimethylformamide / 4.5 h / 20 °C

3: 94 percent / methoxybenzene; dimethylformamide / 5.5 h / 95 - 160 °C

4: 142 mg / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

With ammonium formate; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; dibutyl ether; methoxybenzene; N,N-dimethyl-formamide; 3: Pictet-Spengler condensation / 4: Mitsunobu reaction;
DOI:10.1021/jm0304414