12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

Base Information

Chemical Name:12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester
CAS No.:944238-75-9
Molecular Formula:C₄₀H₄₄O₃
Molecular Weight:572.788
Hs Code.:

Synonyms:12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

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Chemical Property of 12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

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Technology Process of 12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

There total 2 articles about 12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 862260-62-6
4-(10-phenylanthracen-9-yl)benzaldehyde

: 71655-36-2
methyl 12-hydroxydodecanoate

: 944238-75-9
12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

Guidance literature:: With triethylsilane; bismuth(III) chloride; In chloroform; at 20 ℃; for 12h;
DOI:10.1002/chem.200600387

Reference yield:

: 23674-20-6
9-bromo-10-phenylanthracene

: 944238-75-9
12-[4-(10-phenyl-anthracen-9-yl)-benzyloxy]-dodecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / tetrakis(triphenylphosphine)palladium / benzene; H₂O; ethanol / 24 h / Heating

2: 70 percent / BiCl₃; Et₃SiH / CHCl₃ / 12 h / 20 °C

With triethylsilane; bismuth(III) chloride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; chloroform; water; benzene; 1: Suzuki coupling;
DOI:10.1002/chem.200600387