methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside
CAS No.:408497-02-9
Molecular Formula:C₃₂H₄₀O₄S
Molecular Weight:520.733
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

There total 3 articles about methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 100-39-0
benzyl bromide

: 408497-00-7
methyl 6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

: 408497-02-9
methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -60 - 20 ℃;
DOI:10.1081/CAR-100108277

Reference yield:

: 188562-73-4
1,2,3,4-tetra-O-acetyl-6,7,8,9,10-pentadeoxy-L-galacto-decopyranose

: 408497-02-9
methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / trimethylsilyltriflate / CH₂Cl₂ / 24 h

2: 80 percent / NaOMe / methanol / 20 °C

3: 47 percent / NaH / dimethylformamide / -60 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100108277

Reference yield:

: 408496-98-0
methyl 2,3,4-tri-O-acetyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

: 408497-02-9
methyl 2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-1-thio-β-L-galacto-decopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOMe / methanol / 20 °C

2: 47 percent / NaH / dimethylformamide / -60 - 20 °C

With sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100108277