4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

Base Information

Chemical Name:4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide
CAS No.:1384872-19-8
Molecular Formula:C₃₈H₃₀Cl₂N₂O₈S₄
Molecular Weight:841.835
Hs Code.:

Synonyms:4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

Suppliers and Price of 4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

There total 2 articles about 4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 124-41-4
sodium methylate

: 2,2-dichloro-2,2a-dihydro-5,6-dimethoxy-1H,8H-2a-(2-chlorophenyl)azeto[2,1-b][1,3]benzothiazin-1-one

: 1384872-19-8
4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

: 97326-03-9
7-(2-Chloro-phenyl)-2,3-dimethoxy-8,9-dihydro-5-thia-8-aza-benzocycloheptene-6-carboxylic acid methyl ester

: 6,7-dimethoxy-4-methoxycarbonyl-3-(2-chlorophenyl)isoquinoline

Guidance literature:: In methanol; for 3h; Reflux;
DOI:10.1016/j.tet.2012.05.033

Reference yield:

: 91937-60-9
2-(o-chlorophenyl)-6,7-dimethoxy-4H-1,3-benzothiazine

: 1384872-19-8
4,4',5,5'-tetramethoxy-{2,2'-di-[5-methoxycarbonyl-4-(2-chlorophenyl)-2-thiazolyl]}-diphenyl disulfide

: 97326-03-9
7-(2-Chloro-phenyl)-2,3-dimethoxy-8,9-dihydro-5-thia-8-aza-benzocycloheptene-6-carboxylic acid methyl ester

: 6,7-dimethoxy-4-methoxycarbonyl-3-(2-chlorophenyl)isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 1 h / Reflux

2: methanol / 3 h / Reflux

In methanol; toluene; 1: Staudinger reaction;
DOI:10.1016/j.tet.2012.05.033