bis(ethylene)(tricyclohexylphosphine)platinum

Base Information

Chemical Name:bis(ethylene)(tricyclohexylphosphine)platinum
CAS No.:57158-83-5
Molecular Formula:C₂₂H₄₁PPt
Molecular Weight:531.621
Hs Code.:

Synonyms:bis(ethylene)(tricyclohexylphosphine)platinum

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(ethylene)(tricyclohexylphosphine)platinum

Chemical Property:

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Technology Process of bis(ethylene)(tricyclohexylphosphine)platinum

There total 1 articles about bis(ethylene)(tricyclohexylphosphine)platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 12130-66-4
bis(cycloocta-1,5-diene)platinum⁽⁰⁾

: 74-85-1
ethene

: 2622-14-2
tricyclohexylphosphine

: 57158-83-5
bis(ethylene)(tricyclohexylphosphine)platinum

Guidance literature:: In Petroleum ether; C2H4-atmosphere; portionwise addn. of Pt-complex to solvent pre-satd. with C2H4, addn. of 1 equiv. of phosphine (pptn.); N2-atmosphere; decantation, washing (light petroleum); further crop on evapn. of mother liquor and washings (vac.), dissoln. in light petroleum,satn. with C2H4, filtration through Al2O3 (under C2H4) and evapn.; elem . anal.;
DOI:10.1039/DT9780001337

Reference yield: 95.0%

: 57158-83-5
bis(ethylene)(tricyclohexylphosphine)platinum

: 526-86-3
2,3-dimethyl-1,4-benzoquinone

: 77115-61-8
ethylene(5-6-η-2,3-dimethylbenzo-1,4-quinone)(tricyclohexylphosphine)platinum

Guidance literature:: In diethyl ether; carried out under dry nitrogen atm., stirring of mixture for 30 min, at room temp.; ppt. removed from mother-liquor, washed with light petroleum, addn. of washings to mother-liquor, soln. reduced in volume giving additional solid, combined crystals washed with light petroleum, elem. anal.;
DOI:10.1039/DT9810000284

Reference yield: 95.0%

: 57158-83-5
bis(ethylene)(tricyclohexylphosphine)platinum

: 844-51-9
2,5-diphenyl-p-benzoquinone

: 77115-65-2
{Pt(C₆H₂O₂(C₆H₅)2)(C₂H₄)(P(C₆H₁₁)3)}

Guidance literature:: In diethyl ether; carried out under dry nitrogen atm., stirring of mixture for 30 min, at room temp.; ppt. removed from mother-liquor, washed with light petroleum, addn. of washings to mother-liquor, soln. reduced in volume, combined crystals washed with light petroleum, recrystn. from toluene-hexane, elem. anal.;
DOI:10.1039/DT9810000284