4-[(4-METHYLBENZYL)OXY]BENZENECARBOHYDRAZIDE

Base Information

• Chemical Name: 4-[(4-METHYLBENZYL)OXY]BENZENECARBOHYDRAZIDE
• CAS No.: 147807-57-6
• Molecular Formula: C₁₅H₁₆N₂O₂
• Molecular Weight: 256.304
• Mol file: 147807-57-6.mol

Synonyms:4-(4-Methyl-benzyloxy)-benzoic acid hydrazide

Chemical Property of 4-[(4-METHYLBENZYL)OXY]BENZENECARBOHYDRAZIDE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

4-[(4-Methylbenzyl)oxy]benzenecarbohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-[(4-METHYLBENZYL)OXY]BENZENECARBOHYDRAZIDE

There total 3 articles about 4-[(4-METHYLBENZYL)OXY]BENZENECARBOHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-ethoxycarbonylphenoxy-(4'-methylphenyl)-methane (56441-63-5) → 4-(4-Methyl-benzyloxy)-benzoic acid hydrazide (147807-57-6)

Guidance literature:

With hydrazine hydrate; In propan-1-ol; for 48h; Heating;

DOI:10.1021/jm00061a006

Reference yield:

Ethyl 4-hydroxybenzoate (120-47-8) → 4-(4-Methyl-benzyloxy)-benzoic acid hydrazide (147807-57-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, 5 h

2: 95 percent / hydrazine hydrate / propan-1-ol / 48 h / Heating

With sodium hydride; hydrazine hydrate; In propan-1-ol;

DOI:10.1021/jm00061a006

Reference yield:

Ethyl 4-hydroxybenzoate (120-47-8) → 4-(4-Methyl-benzyloxy)-benzoic acid hydrazide (147807-57-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium hydroxide / acetonitrile / 0.5 h / Reflux

1.2: 3 h / Reflux

2.1: hydrazine hydrate / ethanol / 6 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; acetonitrile;

DOI:10.2174/1570180810666131122003939

upstream raw materials:

4-ethoxycarbonylphenoxy-(4'-methylphenyl)-methane

Ethyl 4-hydroxybenzoate

Downstream raw materials:

4-(4-Methyl-benzyloxy)-benzoic acid N'-(2-cyano-ethyl)-hydrazide

C₁₆H₁₄N₂O₃

C₂₀H₂₅N₃O₃

4-butyl-5-(4-(4-methylbenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

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