Technology Process of C34H28N4O4
There total 6 articles about C34H28N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methoxybenzene; trifluoroacetic acid;
for 24h;
DOI:10.1021/ja971304x
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 89 percent / LiBH4 / tetrahydrofuran / 0.33 h
2: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature
3: 85 percent / BF3*OEt2 / diethyl ether / 24 h / 25 - 30 °C
4: 85 percent / NaOAc / aq. ethanol / 0.5 h / Heating
5: 68 percent / KOH, n-Bu4NBr / tetrahydrofuran / 0.5 h
6: 25 percent / anisole, TFA / 24 h
With
potassium hydroxide; lithium borohydride; boron trifluoride diethyl etherate; tetrabutylammomium bromide; sodium acetate; pyridinium trifluroacetate; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; ethanol; dimethyl sulfoxide; benzene;
DOI:10.1021/ja971304x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / BF3*OEt2 / diethyl ether / 24 h / 25 - 30 °C
2: 85 percent / NaOAc / aq. ethanol / 0.5 h / Heating
3: 68 percent / KOH, n-Bu4NBr / tetrahydrofuran / 0.5 h
4: 25 percent / anisole, TFA / 24 h
With
potassium hydroxide; boron trifluoride diethyl etherate; tetrabutylammomium bromide; sodium acetate; methoxybenzene; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/ja971304x
