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Technology Process of C48H46BrCl2N5O12

C48H46BrCl2N5O12

Base Information
  • Chemical Name:C48H46BrCl2N5O12
  • CAS No.:1229117-58-1
  • Molecular Formula:C48H46BrCl2N5O12
  • Molecular Weight:1035.73
  • Hs Code.:
C<sub>48</sub>H<sub>46</sub>BrCl<sub>2</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C48H46BrCl2N5O12

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Chemical Property of C48H46BrCl2N5O12
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Technology Process of C48H46BrCl2N5O12

There total 1 articles about C48H46BrCl2N5O12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C<sub>48</sub>H<sub>47</sub>BrCl<sub>2</sub>N<sub>6</sub>O<sub>12</sub>

C48H47BrCl2N6O12

C<sub>48</sub>H<sub>46</sub>BrCl<sub>2</sub>N<sub>5</sub>O<sub>12</sub>
1229117-58-1

C48H46BrCl2N5O12

Guidance literature:
C48H47BrCl2N6O12; With tert.-butylnitrite; hypophosphorous acid; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
With water; In tetrahydrofuran; ethyl acetate; Inert atmosphere;
DOI:10.1021/ja102304p

Reference yield: 96.0%

(R)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-2-(3,5-dichloro-4-hydroxyphenyl)acetic acid
1027761-55-2

(R)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-2-(3,5-dichloro-4-hydroxyphenyl)acetic acid

C<sub>48</sub>H<sub>46</sub>BrCl<sub>2</sub>N<sub>5</sub>O<sub>12</sub>
1229117-58-1

C48H46BrCl2N5O12

C<sub>66</sub>H<sub>53</sub>BrCl<sub>4</sub>N<sub>6</sub>O<sub>14</sub>
1229117-59-2

C66H53BrCl4N6O14

Guidance literature:
C48H46BrCl2N5O12; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h; Inert atmosphere;
(R)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-2-(3,5-dichloro-4-hydroxyphenyl)acetic acid; With 2,6-dimethylpyridine; HATU; In tetrahydrofuran; dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja102304p
Downstream raw materials:

C66H53BrCl4N6O14

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