5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

Base Information

Chemical Name:5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate
CAS No.:1565622-51-6
Molecular Formula:C₃₅H₂₄N₂O₅
Molecular Weight:552.586
Hs Code.:

Synonyms:5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

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Chemical Property of 5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

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Technology Process of 5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

There total 4 articles about 5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1565621-96-6
2-acetyl-5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]phenyl benzoate

: 100-52-7
benzaldehyde

: 1565622-51-6
5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

Guidance literature:: With potassium hydroxide; In ethanol; at 20 ℃; for 72h;
DOI:10.1007/s00044-014-0938-8

Reference yield:

: 120196-22-7
1-{2,4-dihydroxy-5-[(E)-2-phenyldiazen-1-yl]phenyl}ethan-1-one

: 1565622-51-6
5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 0.5 h

2: potassium hydroxide / ethanol / 72 h / 20 °C

With potassium hydroxide; sodium hydroxide; In ethanol; water;
DOI:10.1007/s00044-014-0938-8

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 1565622-51-6
5-(benzoyloxy)-4-[(E)-2-phenyldiazen-1-yl]-2-[(2E)-3-phenylprop-2-enoyl]phenyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / 0 - 5 °C

1.2: 140 - 150 °C

2.1: sodium hydroxide / water / 0.5 h

3.1: potassium hydroxide / ethanol / 72 h / 20 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium nitrite; In ethanol; water;
DOI:10.1007/s00044-014-0938-8