C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

Base Information

Chemical Name:C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)
CAS No.:147609-51-6
Molecular Formula:C₁₃H₂₃BO₂
Molecular Weight:222.135
Hs Code.:

C<sub>6</sub>H<sub>9</sub>CH<sub>2</sub>B(OC(CH<sub>3</sub>)2C(CH<sub>3</sub>)2O)

Synonyms:C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

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Chemical Property of C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

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Technology Process of C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

There total 2 articles about C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 17497-53-9
1-iodo-1-cyclohexene

: 129422-12-4
((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)zinc(II) iodide

: 147609-51-6
C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

Guidance literature:: Pd*2(C₆H₅HCCH)2CO*4As(C₆H₅)3 = Pd((C₆H₅)HCCHC(O)CHCH(C₆H₅))2*4As(C₆H₅)3; In tetrahydrofuran; heating mixt. of 1 equiv. org. compd., 2 equiv. B-compd. and 0.03 equiv. catalyst in THF (50°C, 3 h);; distn.;;
DOI:10.1016/0022-328X(93)83081-6

Reference yield:

: 4845-04-9
1-cyclohexene-1-methanol

: 73183-34-3
bis(pinacol)diborane

: 147609-51-6
C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

Guidance literature:: With bis[(benzyldimethylamino)chloropalladium(II)]; toluene-4-sulfonic acid; In methanol; dimethyl sulfoxide; at 50 ℃; Inert atmosphere;
DOI:10.1021/ol4019375

Reference yield: 50.0%

: 147609-51-6
C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O)

: 124-38-9,18923-20-1
carbon dioxide

: 859849-88-0
2-methylenecyclohexanecarboxylic acid

Guidance literature:: C₆H₉CH₂B(OC(CH₃)2C(CH₃)2O); carbon dioxide; With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium tert-butylate; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere; Sealed tube;

With hydrogenchloride; In tetrahydrofuran; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/ol4019375