bisebromoamide

Base Information

Chemical Name:bisebromoamide
CAS No.:1191115-30-6
Molecular Formula:C₅₁H₇₂BrN₇O₈S
Molecular Weight:1023.14
Hs Code.:

Synonyms:bisebromoamide

Suppliers and Price of bisebromoamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of bisebromoamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of bisebromoamide

There total 20 articles about bisebromoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1233365-45-1
C₂₈H₃₉BrN₄O₆S

: 1233365-30-4
C₂HF₃O₂*C₂₃H₃₅N₃O₃

: 1191115-30-6
bisebromoamide

Guidance literature:: With 2,3,4-lutidine; 1-hydroxy-7-aza-benzotriazole; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;
DOI:10.1021/ol101021v

Reference yield:

: 1233367-32-2
C₂₄H₃₃BrN₄O₄

: C₂HF₃O₂*C₂₇H₄₂N₄O₄S

: 1191115-30-6
bisebromoamide

Guidance literature:: With sodium hydrogencarbonate; In methanol; at 70 ℃; pH=6; aq. buffer; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.11.058

Reference yield:

: 1301240-79-8
C₂₆H₃₃BrN₂O₅

: 1191115-30-6
bisebromoamide

Guidance literature:: Multi-step reaction with 4 steps

1: water; lithium hydroxide / tetrahydrofuran / 2 h / 0 °C

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran

3: palladium on carbon; hydrogen / ethyl acetate / 24 h / 760.05 Torr

4: sodium hydrogencarbonate / methanol / 70 °C / pH 6 / aq. buffer; Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; palladium on carbon; water; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1016/j.tetlet.2010.11.058