N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

Base Information

Chemical Name:N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide
CAS No.:152171-27-2
Molecular Formula:C₂₉H₃₃ClN₂O₄S₂
Molecular Weight:573.177
Hs Code.:

Synonyms:N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

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Technology Process of N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

There total 8 articles about N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5345-42-6
1-methoxy-3-methyl-2-nitro-benzene

: 152171-27-2
N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: pyrrolidine / dimethylformamide / 24 h / 130 °C

2: H₂ / 10percent Pd/C / 3 h / 2585.7 Torr

3: NaBH₃CN / acetic acid / 0.5 h / Ambient temperature

4: Et₃N / CH₂Cl₂

5: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, 0 deg C, 90 min

With pyrrolidine; hydrogen; tin(IV) chloride; sodium cyanoborohydride; triethylamine; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1080/00397919308013780

Reference yield:

: [(E)-2-(3-Methoxy-2-nitro-phenyl)-vinyl]-dimethyl-amine

: 152171-27-2
N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / 3 h / 2585.7 Torr

2: NaBH₃CN / acetic acid / 0.5 h / Ambient temperature

3: Et₃N / CH₂Cl₂

4: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, 0 deg C, 90 min

With hydrogen; tin(IV) chloride; sodium cyanoborohydride; triethylamine; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1080/00397919308013780

Reference yield:

: 3189-22-8
7-methoxy-1H-indole

: 152171-27-2
N,N-di-n-propyl-(1-benzenesulfonyl-7-methoxy-5-indolinyl)-(p-chlorophenylthio)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₃CN / acetic acid / 0.5 h / Ambient temperature

2: Et₃N / CH₂Cl₂

3: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, 0 deg C, 90 min

With tin(IV) chloride; sodium cyanoborohydride; triethylamine; trifluoroacetic anhydride; In dichloromethane; acetic acid;
DOI:10.1080/00397919308013780