N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

Base Information

Chemical Name:N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide
CAS No.:54042-42-1
Molecular Formula:C₂₅H₁₇ClN₄O₄
Molecular Weight:472.887
Hs Code.:

Synonyms:N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

There total 4 articles about N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 54485-85-7
N-[4-(2-benzoyl-4-chloro-phenyl)-4H-[1,2,4]triazol-3-ylmethyl]-phthalimide

: 54042-42-1
N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

Guidance literature:: In xylene; at 120 - 123 ℃; for 1.58333h;
DOI:10.1002/jhet.5570170331

Reference yield:

: 59010-35-4
1,3-Dioxo-2-isoindolineacetic Acid, <methylene>hydrazine

: 54042-42-1
N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / trifluoroacetic acid / toluene / 1.5 h / 100 - 110 °C

2: 90 percent / xylene / 1.58 h / 120 - 123 °C

With trifluoroacetic acid; In toluene; xylene;
DOI:10.1002/jhet.5570170331

Reference yield:

: 6780-38-7
N-phthaloylglycine chloride

: 54042-42-1
N-<<4-(2-Benzoyl-4-chlorophenyl)-5-(hydroxymethyl)-4H-1,2,4-triazol-3-yl>methyl>phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 90.7 percent / pyridine / tetrahydrofuran / 6 h / 0 - 25 °C

2: 53 percent / trifluoroacetic acid / toluene / 1.5 h / 100 - 110 °C

3: 90 percent / xylene / 1.58 h / 120 - 123 °C

With pyridine; trifluoroacetic acid; In tetrahydrofuran; toluene; xylene;
DOI:10.1002/jhet.5570170331