8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

Base Information

Chemical Name:8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane
CAS No.:951745-27-0
Molecular Formula:C₃₂H₃₃N₃O₄
Molecular Weight:523.632
Hs Code.:

Synonyms:8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

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Chemical Property of 8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

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Technology Process of 8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

There total 6 articles about 8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₇N₃O₃

: 3179-10-0
1-methoxy-4-(2-nitro-vinyl)-benzene

: 951745-27-0
8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

Guidance literature:: In methanol; for 20h;

Reference yield:

: 28957-72-4
N-benzyltropinone

: 951745-27-0
8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen; acetic acid / ASCA-2 / 5 h / 20 °C / 760.05 Torr

2.1: sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / -15 °C

3.2: 15 h / -15 - 20 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 5 h

5.1: methanol / 1.5 h / 20 °C

6.1: methanol / 20 h

With hydrogenchloride; potassium tert-butylate; hydrogen; sodium hydrogencarbonate; acetic acid; ASCA-2; In tetrahydrofuran; methanol; water;

Reference yield:

: 542-05-2
acetonedicarboxylic acid

: 951745-27-0
8-benzyloxycarbonyl-3-(1,5-bis(4-methoxyphenyl)-1H-pyrazol-3-yl)-8-azabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride / water / 2 h / 80 °C

1.2: 14 h / 0 - 55 °C

1.3: 20 °C

2.1: hydrogen; acetic acid / ASCA-2 / 5 h / 20 °C / 760.05 Torr

3.1: sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 20 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / -15 °C

4.2: 15 h / -15 - 20 °C

5.1: hydrogenchloride / tetrahydrofuran; water / 5 h

6.1: methanol / 1.5 h / 20 °C

7.1: methanol / 20 h

With hydrogenchloride; potassium tert-butylate; hydrogen; sodium hydrogencarbonate; acetic acid; ASCA-2; In tetrahydrofuran; methanol; water;