C₃₅H₆₀Cl₂N₂O₂

Base Information

Chemical Name:C₃₅H₆₀Cl₂N₂O₂
CAS No.:1312953-74-4
Molecular Formula:C₃₅H₆₀Cl₂N₂O₂
Molecular Weight:611.78
Hs Code.:

C<sub>35</sub>H<sub>60</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₃₅H₆₀Cl₂N₂O₂

Suppliers and Price of C₃₅H₆₀Cl₂N₂O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₅H₆₀Cl₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₅H₆₀Cl₂N₂O₂

There total 10 articles about C₃₅H₆₀Cl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312953-73-3
C₃₅H₆₂N₂O₄

: 1312953-74-4
C₃₅H₆₀Cl₂N₂O₂

Guidance literature:: With thionyl chloride; In toluene; for 3h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.02.027

Reference yield:

: 204844-09-7
1,1-dicyclohexyl-2-hydroxy ethane

: 1312953-74-4
C₃₅H₆₀Cl₂N₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / methanol; water / 124 h / 20 °C / Inert atmosphere

3.1: sulfuric acid / 18 h / Inert atmosphere; Heating

3.2: 0 °C / Inert atmosphere

4.1: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 70 °C / 4137.29 Torr

5.1: hydrogenchloride; water / ethanol / 20 h / Inert atmosphere; Reflux

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 13 h / 0 °C / Inert atmosphere; Reflux

6.2: 0.5 h / 0 °C / Inert atmosphere; Reflux

7.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: thionyl chloride / toluene / 3 h / Inert atmosphere; Reflux

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; oxalyl dichloride; sulfuric acid; 20 % Pd(OH)2/C; water; hydrogen; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2011.02.027

Reference yield:

: D,L-3,3-dicyclohexylalanine HCl

: 1312953-74-4
C₃₅H₆₀Cl₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 13 h / 0 °C / Inert atmosphere; Reflux

1.2: 0.5 h / 0 °C / Inert atmosphere; Reflux

2.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: thionyl chloride / toluene / 3 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.02.027