4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

Base Information

Chemical Name:4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole
CAS No.:1398230-14-2
Molecular Formula:C₁₄H₁₅BrFNO₂S
Molecular Weight:360.247
Hs Code.:

Synonyms:4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

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Chemical Property of 4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

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Technology Process of 4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

There total 5 articles about 4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1398230-06-2
(2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazol-4-yl)methanol

: 1398230-14-2
4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

Guidance literature:: With hexabromoacetone; triphenylphosphine; In acetonitrile; at 0 - 40 ℃; for 1h; Inert atmosphere;

Reference yield:

: 1398229-90-7
3-(2-fluoroethoxy)-4-methoxybenzothioamide

: 1398230-14-2
4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 2.5 h / Reflux; Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 55 °C / Inert atmosphere

2.2: 0 °C

3.1: triphenylphosphine; hexabromoacetone / acetonitrile / 1 h / 0 - 40 °C / Inert atmosphere

With lithium aluminium tetrahydride; hexabromoacetone; triphenylphosphine; In tetrahydrofuran; ethanol; acetonitrile;

Reference yield:

: 1398229-98-5
ethyl 2-(3-(2-Fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole-4-carboxylate

: 1398230-14-2
4-(bromomethyl)-2-(3-(2-fluoroethoxy)-4-methoxyphenyl)-5-methylthiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 55 °C / Inert atmosphere

1.2: 0 °C

2.1: triphenylphosphine; hexabromoacetone / acetonitrile / 1 h / 0 - 40 °C / Inert atmosphere

With lithium aluminium tetrahydride; hexabromoacetone; triphenylphosphine; In tetrahydrofuran; acetonitrile;