N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

Base Information

Chemical Name:N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide
CAS No.:1501972-49-1
Molecular Formula:C₂₁H₂₇ClN*I
Molecular Weight:455.81
Hs Code.:

Synonyms:N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

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Chemical Property of N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

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Technology Process of N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

There total 5 articles about N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 593-71-5
Chloroiodomethane

: N,N-dimethyl-6,6-diphenyl-5-hexenylamine

: 1501972-49-1
N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

Guidance literature:: In acetonitrile; at 20 ℃; for 24h; Darkness;
DOI:10.3390/molecules21040381

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1501972-49-1
N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / benzene / 6 h / Dean-Stark; Reflux

3: water; tetrahydrofuran / 20 °C

4: acetonitrile / 24 h / 20 °C / Darkness

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; water; acetonitrile; benzene; 1: |Grignard Reaction;
DOI:10.3390/molecules21040381

Reference yield:

: 22809-37-6
6-bromohexanoyl chloride

: 1501972-49-1
N-chloromethyl-N,N-dimethyl-N-(6,6-diphenylhex-5-en-1-yl)ammonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / benzene / 6 h / Dean-Stark; Reflux

3: water; tetrahydrofuran / 20 °C

4: acetonitrile / 24 h / 20 °C / Darkness

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; water; acetonitrile; benzene; 1: |Grignard Reaction;
DOI:10.3390/molecules21040381