Technology Process of C26H35ClO7
There total 14 articles about C26H35ClO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-chloro-succinimide; osmium(VIII) oxide; water;
In
acetone; tert-butyl alcohol;
for 8h;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: silver(l) oxide / dichloromethane / 48 h / 20 °C / Molecular sieve; Inert atmosphere; Darkness
2.1: trifluoroacetic acid; water / acetic acid / 3.5 h / 20 °C
3.1: n-butyllithium / hexane; diethyl ether / 1 h / -78 °C
3.2: 0.17 h / -78 - 0 °C
3.3: 11 h / 10 °C
4.1: trifluoroacetic acid; water / acetic acid / 14 h / 20 °C
5.1: methyllithium / tetrahydrofuran / 0.5 h / -78 °C
5.2: 1 h / -78 °C
5.3: 2 h / -78 - 20 °C
6.1: triethylamine; methanesulfonyl chloride / diethyl ether / 1.33 h / 0 - 20 °C
6.2: 1 h / -35 - 20 °C
7.1: trifluoroacetic acid; water / acetic acid / 1 h / 20 °C
8.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 6 h / 20 °C
8.2: 2 h / 80 °C
9.1: osmium(VIII) oxide; water / tert-butyl alcohol / 0.75 h / 20 °C
10.1: N-chloro-succinimide; osmium(VIII) oxide; water / tert-butyl alcohol; acetone / 8 h
With
N-chloro-succinimide; osmium(VIII) oxide; n-butyllithium; 2,4,6-trichlorobenzoyl chloride; water; methyllithium; methanesulfonyl chloride; triethylamine; trifluoroacetic acid; silver(l) oxide;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetic acid; acetone; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: trifluoroacetic acid; water / acetic acid / 3.5 h / 20 °C
2.1: n-butyllithium / hexane; diethyl ether / 1 h / -78 °C
2.2: 0.17 h / -78 - 0 °C
2.3: 11 h / 10 °C
3.1: trifluoroacetic acid; water / acetic acid / 14 h / 20 °C
4.1: methyllithium / tetrahydrofuran / 0.5 h / -78 °C
4.2: 1 h / -78 °C
4.3: 2 h / -78 - 20 °C
5.1: triethylamine; methanesulfonyl chloride / diethyl ether / 1.33 h / 0 - 20 °C
5.2: 1 h / -35 - 20 °C
6.1: trifluoroacetic acid; water / acetic acid / 1 h / 20 °C
7.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 6 h / 20 °C
7.2: 2 h / 80 °C
8.1: osmium(VIII) oxide; water / tert-butyl alcohol / 0.75 h / 20 °C
9.1: N-chloro-succinimide; osmium(VIII) oxide; water / tert-butyl alcohol; acetone / 8 h
With
N-chloro-succinimide; osmium(VIII) oxide; n-butyllithium; 2,4,6-trichlorobenzoyl chloride; water; methyllithium; methanesulfonyl chloride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; hexane; acetic acid; acetone; toluene; tert-butyl alcohol;