Technology Process of C18H24FNO4
There total 5 articles about C18H24FNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; tert-butyl XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
1,4-dioxane; water;
at 80 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: calcium chloride / methanol / 0.5 h / Cooling with ice
1.2: 1 h
2.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 °C
3.1: potassium hydroxide; tert-butyl XPhos / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 80 °C
With
di-isopropyl azodicarboxylate; triphenylphosphine; calcium chloride; potassium hydroxide; tert-butyl XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
1,4-dioxane; methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water; tetrahydrofuran / 1 h / 20 °C / Cooling with ice
2.1: calcium chloride / methanol / 0.5 h / Cooling with ice
2.2: 1 h
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 °C
4.1: potassium hydroxide; tert-butyl XPhos / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 80 °C
With
di-isopropyl azodicarboxylate; triphenylphosphine; calcium chloride; potassium hydroxide; sodium hydroxide; tert-butyl XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; 1,4-dioxane; methanol; water; toluene;