iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

Base Information

Chemical Name:iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate
CAS No.:1252813-50-5
Molecular Formula:C₂₀H₃₁BO₄
Molecular Weight:346.275
Hs Code.:

Synonyms:iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

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Technology Process of iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

There total 2 articles about iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 31416-75-8
Isobutyl-p-methylcinnamat

: 73183-34-3
bis(pinacol)diborane

: 1252813-50-5
iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

Guidance literature:: With sodium t-butanolate; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I)chloride; In methanol; diethyl ether; at -55 ℃; for 6h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 53801-42-6
(E)-isobutyl 3-(p-tolyl)acrylate

: 73183-34-3
bis(pinacol)diborane

: iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

: 1252813-50-5
iso-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-p-tolylpropanoate

Guidance literature:: With methanol; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I) chloride; sodium t-butanolate; In toluene; at -55 ℃; for 6h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol1021756