3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

Base Information

Chemical Name:3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose
CAS No.:1143578-54-4
Molecular Formula:C₃₉H₄₁NO₁₀
Molecular Weight:683.755
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

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Chemical Property of 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

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Technology Process of 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

There total 1 articles about 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3868-03-9
1,6:2,3-dianhydro-β-D-mannopyranose

: 1143578-50-0
C₃₅H₃₅Cl₃N₂O₇

: 1143578-54-4
3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

Guidance literature:: 1,6:2,3-dianhydro-β-D-mannopyranose; C₃₅H₃₅Cl₃N₂O₇; In dichloromethane; acetonitrile; for 2h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 70.0%

: 1143578-54-4
3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose

: 1143578-62-4
C₃₃H₃₄N₄O₆

: 1143578-63-5
C₃₉H₄₂N₄O₁₀

: 1143578-82-8
C₃₉H₄₂N₄O₁₀

: 645-59-0
dihydrocinnamonitrile

Guidance literature:: 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranosyl-(1->4)-1,6:2,3-dianhydro-β-D-mannopyranose; With trimethylsilylazide; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 21.5h; Reflux; Inert atmosphere;

In acetonitrile; mineral oil;