Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

Base Information

Chemical Name:Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester
CAS No.:423764-49-2
Molecular Formula:C₁₃H₁₉BrO₂
Molecular Weight:287.197
Hs Code.:

Synonyms:Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

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Chemical Property of Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

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Technology Process of Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

There total 1 articles about Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 590-15-8
trans-2-propenyl bromide

: 50870-61-6
2-bromocyclohex-2-en-1-one

: 141-75-3
butyryl chloride

: 423764-49-2
Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

Guidance literature:: trans-2-propenyl bromide; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.25h;

2-bromocyclohex-2-en-1-one; In tetrahydrofuran; pentane; at -78 - 0 ℃;

butyryl chloride; In tetrahydrofuran; pentane; at 0 - 20 ℃; Further stages.;
DOI:10.1021/jo010752r

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 423764-49-2
Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

: {(Z)-1-[2-Bromo-1-((E)-propenyl)-cyclohex-2-enyloxy]-but-1-enyloxy}-triisopropyl-silane

Guidance literature:: triisopropylsilyl trifluoromethanesulfonate; Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester; With potassium hexamethylsilazane; In diethyl ether; at -78 ℃;

With acetic acid; In diethyl ether; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo010752r

Reference yield:

: 423764-49-2
Butyric acid 2-bromo-1-((E)-propenyl)-cyclohex-2-enyl ester

: (2S,3S)-4-[2-Bromo-cyclohex-2-en-(E)-ylidene]-2-ethyl-3-methyl-butyric acid

: (2R,3S)-4-[2-Bromo-cyclohex-2-en-(E)-ylidene]-2-ethyl-3-methyl-butyric acid

Guidance literature:: With tetrabutyl ammonium fluoride; triisopropylsilyl trifluoromethanesulfonate; potassium hexamethylsilazane; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃;
DOI:10.1016/S0040-4020(01)00349-0