4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide

Base Information

• Chemical Name: 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide
• CAS No.: 1006906-81-5
• Molecular Formula: C₁₈H₁₉FN₄O₃S
• Molecular Weight: 390.438

Synonyms:4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide

Chemical Property of 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide

Chemical Property:

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Technology Process of 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide

There total 2 articles about 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethoxy-2-iminoethyl 2-(2,5-dimethylphenyl)acetate hydrochloride (1034471-81-2) + 3-fluoro-4-hydrazino-1-benzenesulfonamide hydrochloride (252561-98-1) → 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide (1006906-81-5)

Guidance literature:

With pyridine; at 70 - 80 ℃; Molecular sieve;

Reference yield:

→ 4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide (1006906-81-5)

Guidance literature:

Reference yield: 100.0%

4-[5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl]-3-fluorobenzenesulfonamide (1006906-81-5) + tert-butyldimethylsilyl chloride (18162-48-6) → {4-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-1-yl]-3-fluorophenyl}sulfonamide (1034471-97-0)

Guidance literature:

With 1H-imidazole; for 16h;

upstream raw materials:

2-ethoxy-2-iminoethyl 2-(2,5-dimethylphenyl)acetate hydrochloride

3-fluoro-4-hydrazino-1-benzenesulfonamide hydrochloride

Downstream raw materials:

(E,Z)-N'-(4-(5-(2,5-dimethylbenzyl)-3-(hydroxymethyl)-1H-1,2,4-triazol-1-yl)-3-fluorophenylsulfonyl)-N,N-dimethylformamidine

{4-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-1-yl]-3-fluorophenyl}sulfonamide

[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl 4-nitrophenyl carbonate

[1-[4-(aminosulfonyl)-2-fluorophenyl]-5-(2,5-dimethylbenzyl)-1H-1,2,4-triazol-3-yl]methyl 6-bromo-hexanoate

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