2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

Base Information

Chemical Name:2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon
CAS No.:77914-24-0
Molecular Formula:C₁₇H₁₉NO₃
Molecular Weight:285.343
Hs Code.:

Synonyms:2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

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Chemical Property of 2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

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Technology Process of 2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

There total 8 articles about 2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77914-23-9
2-(4-Hydroxy-3-nitrophenyl)-p-methoxybutyrophenon

: 77914-24-0
2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

Guidance literature:: With sodium hydroxide; sodium dithionite; In acetone;
DOI:10.1002/ardp.19813140312

Reference yield:

: 6973-78-0
2-(4-Nitrophenyl)-buttersaeureethylester

: 77914-24-0
2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / 80-100percent hydrazine hydrate / Raney Ni / ethanol / 1 h / Heating

3: NaNO₂, acetic acid / 5 h

4: SOCl₂ / 2 h / Heating

5: AlCl₃ / CS₂ / 2.5 h

6: 90 percent / aq. NaOH, Na₂S₂O₄ / acetone

With sodium hydroxide; aluminium trichloride; thionyl chloride; sodium dithionite; hydrazine hydrate; acetic acid; sodium nitrite; nickel; In carbon disulfide; ethanol; acetone;
DOI:10.1002/ardp.19813140312

Reference yield:

: 119-43-7
ethyl 2-phenylbutanoate

: 77914-24-0
2-(3-Amino-4-hydroxyphenyl)-p-methoxybutyrophenon

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / conc. H₂SO₄, HNO₃ / 2 h

2: 97 percent / 80-100percent hydrazine hydrate / Raney Ni / ethanol / 1 h / Heating

4: NaNO₂, acetic acid / 5 h

5: SOCl₂ / 2 h / Heating

6: AlCl₃ / CS₂ / 2.5 h

7: 90 percent / aq. NaOH, Na₂S₂O₄ / acetone

With sodium hydroxide; aluminium trichloride; thionyl chloride; sodium dithionite; sulfuric acid; nitric acid; hydrazine hydrate; acetic acid; sodium nitrite; nickel; In carbon disulfide; ethanol; acetone;
DOI:10.1002/ardp.19813140312