C₂₂H₂₃⁽²⁾HO₆

Base Information

• Chemical Name: C₂₂H₂₃⁽²⁾HO₆
• CAS No.: 207348-97-8
• Molecular Formula: C₂₂H₂₄O₆
• Molecular Weight: 385.421
• Mol file: 207348-97-8.mol

Synonyms:C₂₂H₂₃⁽²⁾HO₆

Chemical Property of C₂₂H₂₃⁽²⁾HO₆

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₂H₂₃⁽²⁾HO₆

There total 1 articles about C₂₂H₂₃⁽²⁾HO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzoyl chloride (98-88-4) + C15H19(2)HO5 → C22H23(2)HO6 (207348-97-8)

Guidance literature:

DOI:10.1016/S0040-4039(98)00433-X

Reference yield: 99.0%

C22H23(2)HO6 (207348-97-8) → C15H17(2)HO6 (207348-99-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid;

DOI:10.1016/S0040-4039(98)00433-X

Reference yield:

C22H23(2)HO6 (207348-97-8) → C22H21(2)HO7 (207349-04-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / H₂ / Pd/C / acetic acid

2: 1.) PDC, molecular sieves 4A, 2.) NaBH₄ / 1.) AcOH, CH₂Cl₂, 2.) MeOH

3: 95 percent

With sodium tetrahydroborate; dipyridinium dichromate; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In acetic acid;

DOI:10.1016/S0040-4039(98)00433-X

upstream raw materials:

benzoyl chloride

Downstream raw materials:

C₁₅H₁₇⁽²⁾HO₆

C₂₂H₂₁⁽²⁾HO₇

C₁₅H₁₇⁽²⁾HO₆