N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin

Base Information

• Chemical Name: N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin
• CAS No.: 89480-40-0
• Molecular Formula: C₇₈H₉₄ClN₁₀O₁₃PSi₃
• Molecular Weight: 1530.35

Synonyms:N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin

Chemical Property of N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin

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Technology Process of N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin

There total 2 articles about N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N6-benzoyl-2',3'-bis-O-<(1,1-dimethylethyl)dimethylsilyl>adenosine (79974-68-8) + Triaethylammonium-6-benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosin-3'-(2-chlorphenyl)phosphat> (75082-92-7) → N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin (89480-40-0)

Guidance literature:

With TPS-NI; In pyridine; for 120h; Ambient temperature;

DOI:10.1002/hlca.19830660713

Reference yield:

5-nitrobenzotriazole (2338-12-7) + N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine (69504-09-2) + N6-benzoyl-2',3'-bis-O-<(1,1-dimethylethyl)dimethylsilyl>adenosine (79974-68-8) + 2-chlorophenyl dichlorophosphate (15074-54-1) → N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2',3'-bis-O-(tert-butyldimethylsilyl)adenosin (89480-40-0)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1246/cl.1987.775

upstream raw materials:

5-nitrobenzotriazole

N⁶-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine

N⁶-benzoyl-2',3'-bis-O-<(1,1-dimethylethyl)dimethylsilyl>adenosine

2-chlorophenyl dichlorophosphate

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