3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

Base Information

Chemical Name:3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide
CAS No.:1235471-28-9
Molecular Formula:C₁₆H₈BrCl₃N₂O₂
Molecular Weight:446.515
Hs Code.:

Synonyms:3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

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Chemical Property of 3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

Chemical Property:

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Technology Process of 3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

There total 7 articles about 3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: C₁₀H₃Cl₄NO₂

: 106-40-1
4-bromo-aniline

: 1235471-28-9
3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

Guidance literature:: With triethylamine; In toluene; at 20 ℃; Reflux;
DOI:10.1007/s00706-010-0265-9

Reference yield:

: 886967-66-4
ethyl 3-(2,3,6-trichlorophenyl)-4,5-dihydroisoxazole-5-carboxylate

: 1235471-28-9
3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide

2: water; sodium hydroxide / ethanol

3: oxalyl dichloride / benzene

4: triethylamine / toluene / 20 °C / Reflux

With N-Bromosuccinimide; oxalyl dichloride; water; triethylamine; sodium hydroxide; In ethanol; toluene; benzene;
DOI:10.1007/s00706-010-0265-9

Reference yield:

: 1235471-16-5
C₁₀H₄Cl₃NO₃

: 1235471-28-9
3-(2,3,6-trichlorophenyl)isoxazole-5-carboxylic acid 4-bromophenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / benzene

2: triethylamine / toluene / 20 °C / Reflux

With oxalyl dichloride; triethylamine; In toluene; benzene;
DOI:10.1007/s00706-010-0265-9