2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:518975-30-9
Molecular Formula:C₇₁H₆₂Cl₃NO₂₂
Molecular Weight:1387.63
Hs Code.:

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 7 articles about 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 518975-30-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 810 mg / pyridine / 20 °C

2: PdCl₂; sodium acetate / acetic acid; H₂O / 12 h

3: 1.01 g / DBU / CH₂Cl₂ / 2 h

With pyridine; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1081/CAR-120016856

Reference yield:

: 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-L-rhamnopyranose

: 518975-30-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 5 steps

1: 876 mg / DBU / CH₂Cl₂ / 2 h

2: TMSOTf / CH₂Cl₂ / 3 h / -25 - 20 °C

3: 810 mg / pyridine / 20 °C

4: PdCl₂; sodium acetate / acetic acid; H₂O / 12 h

5: 1.01 g / DBU / CH₂Cl₂ / 2 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1081/CAR-120016856

Reference yield:

: 518975-27-4
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

: 518975-30-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->2)-3-O-acetyl-4-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: TMSOTf / CH₂Cl₂ / 3 h / -25 - 20 °C

2: 810 mg / pyridine / 20 °C

3: PdCl₂; sodium acetate / acetic acid; H₂O / 12 h

4: 1.01 g / DBU / CH₂Cl₂ / 2 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1081/CAR-120016856