1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

Base Information

Chemical Name:1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion
CAS No.:156304-65-3
Molecular Formula:C₂₂H₂₇N₃O₃
Molecular Weight:381.475
Hs Code.:

Synonyms:1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

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Chemical Property of 1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

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Technology Process of 1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

There total 1 articles about 1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 15988-11-1
4-Phenylurazole

: 3315-32-0,2525-39-5
2,4,6-tri-tert-butylphenoxyl

: 156304-65-3
1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

: 1,2-Bis-(3,5-di-tert-butyl-2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

Guidance literature:: In benzene; at 50 ℃; for 4h;
DOI:10.1002/prac.19943360414

Reference yield:

: 156304-65-3
1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

: C₂₂H₂₅N₃O₃

Guidance literature:: With lead(IV) acetate; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1021/ja00006a059

Reference yield:

: 156304-65-3
1-(3,5-Di-tert-butyl2-hydroxy-1-phenyl)-4-phenyl-1,2,4-triazolidin-3,5-dion

: 132207-20-6
5-(3,5-Di-tert-butyl-6-oxo-cyclohexa-2,4-dienylidene)-2,2-dimethyl-[1,3]dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: LTA / tetrahydrofuran / 1 h / -78 °C

2: Et₃N / tetrahydrofuran / 0.25 h / 0 °C

With lead(IV) acetate; triethylamine; In tetrahydrofuran;
DOI:10.1021/ja00006a059