C₄₀H₄₉N₉O₆S₂

Base Information

Chemical Name:C₄₀H₄₉N₉O₆S₂
CAS No.:1453168-03-0
Molecular Formula:C₄₀H₄₉N₉O₆S₂
Molecular Weight:816.018
Hs Code.:

C<sub>40</sub>H<sub>49</sub>N<sub>9</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₄₀H₄₉N₉O₆S₂

Suppliers and Price of C₄₀H₄₉N₉O₆S₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₀H₄₉N₉O₆S₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₀H₄₉N₉O₆S₂

There total 12 articles about C₄₀H₄₉N₉O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1453167-97-9
C₄₈H₅₅N₉O₈S₂

: 1453168-03-0
C₄₀H₄₉N₉O₆S₂

Guidance literature:: With hydrogen bromide; acetic acid; for 1h;
DOI:10.1021/ol401749p

Reference yield:

: 19901-50-9,51987-73-6,77119-84-7
methyl (2R)-2-(t-butoxycarbonylamino)-3-phenylpropionate

: 1453168-03-0
C₄₀H₄₉N₉O₆S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: ammonium hydroxide / methanol

2.1: Lawessons reagent / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

3.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 0.25 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

3.3: 0 - 20 °C / Inert atmosphere

4.1: trifluoroacetic acid; methoxybenzene / dichloromethane

5.1: N-ethyl-N,N-diisopropylamine; HATU; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid; methoxybenzene / dichloromethane

7.1: N-ethyl-N,N-diisopropylamine; HATU; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 1 h / 20 °C / Inert atmosphere

8.1: lithium hydroxide; dihydrogen peroxide / ethanol

9.1: trifluoroacetic acid; methoxybenzene / dichloromethane

10.1: N-ethyl-N,N-diisopropylamine; HATU; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 1 h / 20 °C / Inert atmosphere

11.1: hydrogen bromide; acetic acid / 1 h

With Lawessons reagent; ammonium hydroxide; hydrogen bromide; dihydrogen peroxide; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; methoxybenzene; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;
DOI:10.1021/ol401749p

Reference yield:

: (R)-tert-butyl 1-amino-3-phenyl-1-thioxopropan-2-ylcarbamate

: 1453168-03-0
C₄₀H₄₉N₉O₆S₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 0.25 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

1.3: 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid; methoxybenzene / dichloromethane

3.1: N-ethyl-N,N-diisopropylamine; HATU; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid; methoxybenzene / dichloromethane

5.1: N-ethyl-N,N-diisopropylamine; HATU; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide; dihydrogen peroxide / ethanol

7.1: trifluoroacetic acid; methoxybenzene / dichloromethane

8.1: N-ethyl-N,N-diisopropylamine; HATU; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 1 h / 20 °C / Inert atmosphere

9.1: hydrogen bromide; acetic acid / 1 h

With hydrogen bromide; dihydrogen peroxide; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; methoxybenzene; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In 1,2-dimethoxyethane; ethanol; dichloromethane;
DOI:10.1021/ol401749p