2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate

Base Information

Chemical Name:2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate
CAS No.:1609373-98-9
Molecular Formula:C₁₃H₈F₃NO₄S
Molecular Weight:331.272
Hs Code.:
Mol file:1609373-98-9.mol

Synonyms:2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

Suppliers and Price of 2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
250mg
$ 77.00

Arctom
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
100mg
$ 45.00

Arctom
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
1g
$ 205.00

Ambeed
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
250mg
$ 78.00

Ambeed
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
100mg
$ 45.00

Ambeed
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
1g
$ 207.00

Ambeed
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98%
5g
$ 702.00

AK Scientific
2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate
1g
$ 374.00

Total 25 raw suppliers

Chemical Property of 2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate

Chemical Property:

Boiling Point:412.0±45.0 °C(Predicted)
PKA:3.13±0.40(Predicted)
Density:1.567±0.06 g/cm3(Predicted)
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

2-Methylbenzofuro[2,3-b]pyridin-8-yltrifluoromethanesulfonate 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate

There total 12 articles about 2-Methylbenzofuro[2,3-b]pyridin-8-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1609373-97-8
2-methylbenzofuro[2,3-b]pyridine-8-ol

: 1609373-98-9
2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃;

Reference yield:

: 1609373-96-7
8-methoxy-2-methylbenzofuro[2,3-b]pyridine

: 1609373-98-9
2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 15 h / 200 °C

2: pyridine / dichloromethane / 0 °C

With pyridine; pyridine hydrochloride; In dichloromethane;

Reference yield:

: 1824-81-3
2-Amino-6-methylpyridine

: 1609373-98-9
2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 7 steps

1: N-Bromosuccinimide / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: iodine / tetrahydrofuran / 17 h / 55 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; water / 90 - 100 °C

4: palladium on activated charcoal; hydrogen / methanol / 20 - 30 °C / 1500.15 - 2250.23 Torr

5: acetic acid; isopentyl nitrite / 0 - 10 °C / Inert atmosphere

6: boron tribromide / dichloromethane / 0 - 25 °C / Inert atmosphere

7: triethylamine / dichloromethane / 0 - 30 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; hydrogen; iodine; boron tribromide; sodium carbonate; acetic acid; triethylamine; isopentyl nitrite; In tetrahydrofuran; methanol; dichloromethane; water; toluene;