2-ethyl isothiocyanate

Base Information

Chemical Name:2-ethyl isothiocyanate
CAS No.:199522-67-3
Molecular Formula:C₁₅H₁₂BrCl₂N₃S
Molecular Weight:417.156
Hs Code.:

2-<N-(5-bromopyrid-2-yl)-N-(3,4-dichlorobenzyl)amino>ethyl isothiocyanate

Synonyms:2-ethyl isothiocyanate

Suppliers and Price of 2-ethyl isothiocyanate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-ethyl isothiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-ethyl isothiocyanate

There total 4 articles about 2-ethyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75-15-0,12122-00-8
carbon disulfide

: 207276-79-7
N-1-(5-bromopyrid-2-yl)-1-(3,4-dichlorobenzyl)ethane-1,2-diamine

: 199522-67-3
2-ethyl isothiocyanate

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm980118e

Reference yield:

: 624-28-2
2,5-dibromopyridine

: 199522-67-3
2-ethyl isothiocyanate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / pyridine / 18 h / Heating

2: 1.) NaH / 1.) DMSO, 2 h, 2.) DMSO, RT, overnight

3: 78 percent / DCC / tetrahydrofuran / Ambient temperature

With pyridine; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm980118e

Reference yield:

: 199522-66-2
N¹-(5-bromopyridin-2-yl)ethane-1,2-diamine

: 199522-67-3
2-ethyl isothiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMSO, 2 h, 2.) DMSO, RT, overnight

2: 78 percent / DCC / tetrahydrofuran / Ambient temperature

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm980118e