((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

Base Information

Chemical Name:((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)
CAS No.:260391-64-8
Molecular Formula:C₂₉H₃₆N₄O₁₂
Molecular Weight:632.624
Hs Code.:

Synonyms:((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

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Chemical Property of ((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

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Technology Process of ((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

There total 3 articles about ((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₁₉H₁₆Cl₂N₂O₁₀

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 260391-64-8
((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

Guidance literature:: With triethylamine; In dichloromethane; at -40 ℃; for 1h;

Reference yield: 65.0%

: 140658-45-3
1',3'-bis(4-carboxy-2-methoxy-5-nitrophenoxy)propane

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 260391-64-8
((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

Guidance literature:: 1',3'-bis(4-carboxy-2-methoxy-5-nitrophenoxy)propane; With oxalyl dichloride; In tetrahydrofuran; acetonitrile; for 24h;

(S)-1-Pyrrolidin-2-yl-methanol; With potassium carbonate; In acetonitrile; at -25 ℃;
DOI:10.1016/S0960-894X(00)00404-2

Reference yield:

: 140658-45-3
1',3'-bis(4-carboxy-2-methoxy-5-nitrophenoxy)propane

: 260391-64-8
((propane-1,3-diylbis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(((S)-2-(hydroxymethyl)pyrrolidin-1-yl)methanone)

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 16 h / 20 °C

2: triethylamine / dichloromethane / 1 h / -40 °C

With oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;