C₆₆H₉₆O₅Si₃

Base Information

Chemical Name:C₆₆H₉₆O₅Si₃
CAS No.:476195-64-9
Molecular Formula:C₆₆H₉₆O₅Si₃
Molecular Weight:1053.74
Hs Code.:

C<sub>66</sub>H<sub>96</sub>O<sub>5</sub>Si<sub>3</sub>

Synonyms:C₆₆H₉₆O₅Si₃

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Chemical Property of C₆₆H₉₆O₅Si₃

Chemical Property:

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Technology Process of C₆₆H₉₆O₅Si₃

There total 11 articles about C₆₆H₉₆O₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 476195-64-9
C₆₆H₉₆O₅Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-BuLi / diethyl ether; hexane / 3 h / -78 °C

1.2: diethyl ether; hexane / -78 - 20 °C

2.1: n-BuLi / diethyl ether; hexane / 2.5 h / -78 °C

2.2: 5.82 g / tetrahydrofuran; hexane / 1.67 h / -78 - 20 °C

3.1: 95 percent / K₂CO₃ / dimethylformamide / 14 h / 70 °C

4.1: 99 percent / ICl / CH₂Cl₂ / 2 h / 20 °C

5.1: Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 2.67 h / 20 - 50 °C

6.1: 3.15 g / Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 16 h / 70 °C

With copper(l) iodide; n-butyllithium; Iodine monochloride; potassium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; triethylamine; In diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; 5.1: Sonogashira coupling / 6.1: Sonogashira coupling;
DOI:10.1021/jo025723a

Reference yield:

: 75894-93-8
1,3-dibromo-5-(2-hydroxyethyl)benzene

: 476195-64-9
C₆₆H₉₆O₅Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: 11.70 g / imidazole / CH₂Cl₂ / 2.5 h / 20 °C

2: 82 percent / Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 48 h / 65 °C

3: 100 percent / K₂CO₃ / CH₂Cl₂; methanol / 2 h / 20 °C

4: Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 2.67 h / 20 - 50 °C

5: 3.15 g / Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 16 h / 70 °C

With 1H-imidazole; copper(l) iodide; potassium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; triethylamine; In methanol; dichloromethane; 2: Sonogashira coupling / 4: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1021/jo025723a

Reference yield:

: 184769-87-7
3,5-dibromo-4-aminophenethyl alcohol

: 476195-64-9
C₆₆H₉₆O₅Si₃

Guidance literature:: Multi-step reaction with 6 steps

1: isoamyl nitrite / dimethylformamide / 0.83 h / 70 °C

2: 11.70 g / imidazole / CH₂Cl₂ / 2.5 h / 20 °C

3: 82 percent / Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 48 h / 65 °C

4: 100 percent / K₂CO₃ / CH₂Cl₂; methanol / 2 h / 20 °C

5: Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 2.67 h / 20 - 50 °C

6: 3.15 g / Pd(dibenzylideneacetone)2; triphenylphosphine; CuI / triethylamine / 16 h / 70 °C

With 1H-imidazole; copper(l) iodide; potassium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; isopentyl nitrite; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; 3: Sonogashira coupling / 5: Sonogashira coupling / 6: Sonogashira coupling;
DOI:10.1021/jo025723a