2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane

Base Information

• Chemical Name: 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane
• CAS No.: 140407-92-7
• Molecular Formula: C₁₉H₂₈O
• Molecular Weight: 272.431
• Mol file: 140407-92-7.mol

Synonyms:2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane

Chemical Property of 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane

There total 3 articles about 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl-triphenylphosphonium iodide (2065-66-9) + 2-(4-methoxy-3-methylphenylethyl)-3,3-dimethylcyclohexan-1-one (123083-83-0) → 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane (140407-92-7)

Guidance literature:

With sodium tert-pentoxide; In toluene;

DOI:10.1016/S0040-4039(00)92335-9

Reference yield:

4-carbethoxy-3-methyl-2-cyclohexen-1-one (487-51-4) → 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane (140407-92-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 98 percent / sodium t-pentoxide / toluene

With sodium tert-pentoxide; In toluene;

DOI:10.1016/S0040-4039(00)92335-9

Reference yield:

2-(3-methyl-4-methoxyphenyl)ethyl bromide (69919-95-5) → 2-(4-methoxy-3-methylphenetyl)-3,3-dimethyl-1-methylenecyclohexane (140407-92-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 98 percent / sodium t-pentoxide / toluene

With sodium tert-pentoxide; In toluene;

DOI:10.1016/S0040-4039(00)92335-9

upstream raw materials:

methyl-triphenylphosphonium iodide

2-(4-methoxy-3-methylphenylethyl)-3,3-dimethylcyclohexan-1-one

4-carbethoxy-3-methyl-2-cyclohexen-1-one

2-(3-methyl-4-methoxyphenyl)ethyl bromide

Downstream raw materials:

<2-(4-methoxy-3-methylphenethyl)3,3-dimethylcyclohexyl>methanol

2-[2-(4-Methoxy-3-methyl-phenyl)-ethyl]-3,3-dimethyl-cyclohexanecarboxylic acid

methyl 2-(4-methoxy-3-methylphenethyl)-3,3-dimethylcyclohexanecarboxylate