Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Base Information

Chemical Name:Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid
CAS No.:74995-86-1
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:

Synonyms:Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Chemical Property:

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Technology Process of Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

There total 7 articles about Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 74995-85-0
Methyl-4-O-benzoyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosid

: 74995-86-1
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Guidance literature:: With pyridine; thionyl chloride; at 0 ℃;
DOI:10.1016/S0040-4039(01)85568-4

Reference yield: 15.0%

: 74995-85-0
Methyl-4-O-benzoyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosid

: 74995-86-1
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

: 78013-83-9,100017-88-7
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methylen-α-D-erythro-hexopyranosid

Guidance literature:: With thionyl chloride; In pyridine; benzene;

Reference yield:

: 6752-52-9,13264-07-8,18424-64-1,19231-32-4,77481-74-4,77481-75-5,77481-76-6,77481-77-7,78086-67-6,100100-70-7
Methyl-4,6-O-benzyliden-2-desoxy-3-C-methyl-α-D-ribo-hexopyranosid

: 74995-86-1
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: N-bromosuccinimide, BaCO₃ / CCl₄ / 2 h / Heating

2: 83 percent / Et₃N, H₂ / Raney-Ni / methanol / 2942.03 Torr

3: 85 percent / SOCl₂ / benzene; pyridine / 3 h / 5 °C

With N-Bromosuccinimide; thionyl chloride; hydrogen; triethylamine; barium carbonate; nickel; In pyridine; methanol; tetrachloromethane; benzene;