4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Base Information

Chemical Name:4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid
CAS No.:99922-58-4
Molecular Formula:C₂₈H₃₀O₇
Molecular Weight:478.542
Hs Code.:

4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

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Technology Process of 4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

There total 2 articles about 4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 74995-86-1
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

: 79607-54-8
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-β-D-erythro-hex-2-enopyranose

: 79607-51-5
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranose

: 99922-58-4,99922-59-5
4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Guidance literature:: With acetic acid; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1002/jlac.198619860402

Reference yield: 5.0%

: 99922-56-2
Methyl-4-O-benzoyl-2,6-didesoxy-3-C-methyl-α-L-ribo-hexopyranosid

: 100017-87-6
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-L-erythro-hex-2-enopyranosid

: 100017-88-7
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methylen-α-L-erythro-hexopyranosid

: 99922-58-4,99922-59-5
4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

Guidance literature:: With pyridine; thionyl chloride; In benzene; at 5 ℃; for 3h;
DOI:10.1002/jlac.198619860402

Reference yield:

: 99922-58-4,99922-59-5
4-O-Benzoyl-1-O-(4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl)-2,3,6-tridesoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosid

: 100017-91-2
Methyl-4-O-benzoyl-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hex-2-enopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: CF₃COOH, CH₃OH / 10 h / -20 deg C to RT

2: 68 percent / 2N NaOH / ethanol / 16 h / Ambient temperature

3: 64 percent / (C₆H₅)3P, ethyl azodicarboxylate / benzene / 2 h / Ambient temperature

With methanol; sodium hydroxide; ethyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In ethanol; benzene;
DOI:10.1002/jlac.198619860402