[Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2

Base Information

• Chemical Name: [Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2
• CAS No.: 188748-24-5
• Molecular Formula: C₂₈H₂₄N₄O₆Pd₂
• Molecular Weight: 725.362

Synonyms:[Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2

Chemical Property of [Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2

Chemical Property:

Purity/Quality:

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Technology Process of [Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2

There total 1 articles about [Pd(CH₃COO)(NC₆H₅)(NOC₆H₄)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

Pd4(μ-CO)4(μ-OCOCH3)4 + Nitrosobenzene (586-96-9) → [Pd(CH3COO)(NC6H5)(NOC6H4)]2 (188748-24-5)

Guidance literature:

In toluene; byproducts: CO2, azoxybenzene; Ar-atmosphere; stirring Pd-complex with 4 equiv. of PhNO (60°C, 3-4 h); filtration, concn., pptn. on hexane addn., collection (filtration), drying (vac.); elem. anal.;

DOI:10.1016/S0022-328X(97)00441-5

Reference yield:

[Pd(CH3COO)(NC6H5)(NOC6H4)]2 (188748-24-5) → palladium (7440-05-3)

Guidance literature:

With hydrogen; In not given; byproducts: CH3COOH, aniline, cyclohexanone; at 20°C and the gas pressure of 1 atm in benzene or toluene soln.; cyclohexane and N2 as by-products; GLC and GLC-mass spectrometry;

DOI:10.1023/A:1013015425154

Reference yield:

[(C6H4(NO)N(C6H5))Pd(CH3COO)2Pd(N(C6H5)C6H4(NO))] (188748-24-5) → palladium (7440-05-3)

Guidance literature:

With carbon monoxide; In not given; byproducts: CH3COOH, phenyl isocyanate, CO2; soln. of Pd complex in benzene or toluene stirred under CO atmosphere (1atm); mechanism discussed; detected by GLC and GLC-MS;

DOI:10.1023/A:1022151806085

upstream raw materials:

Nitrosobenzene

Downstream raw materials:

palladium

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