2-(N,N-dimethylamino)hexyl hydrogen fumarate

Base Information

Chemical Name:2-(N,N-dimethylamino)hexyl hydrogen fumarate
CAS No.:263911-14-4
Molecular Formula:C₁₂H₂₁NO₄
Molecular Weight:243.303
Hs Code.:

Synonyms:2-(N,N-dimethylamino)hexyl hydrogen fumarate

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Chemical Property of 2-(N,N-dimethylamino)hexyl hydrogen fumarate

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Technology Process of 2-(N,N-dimethylamino)hexyl hydrogen fumarate

There total 1 articles about 2-(N,N-dimethylamino)hexyl hydrogen fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 108-31-6
maleic anhydride

: 1862-07-3
6-(N,N-dimethylamino)-1-hexanol

: 263911-14-4
2-(N,N-dimethylamino)hexyl hydrogen fumarate

Guidance literature:: In toluene; for 6h; Heating;
DOI:10.1021/ja9940571

Reference yield:

: 263911-14-4
2-(N,N-dimethylamino)hexyl hydrogen fumarate

: trans-1-[6-(N,N-dimethylamino)hexylthio]-2-(dimethyloctylsilyl)-4-(octanoxycarbonyl)-5-[6-(N,N-dimethylamino)hexanoxycarbonyl]-1-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 24 h

2: 34 percent / 4-tert-butylcatechol / toluene / 24 h / 85 °C

With dmap; 4-tert-Butylcatechol; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Esterification / 2: Diels-Alder reaction;
DOI:10.1021/ja9940571

Reference yield:

: 263911-14-4
2-(N,N-dimethylamino)hexyl hydrogen fumarate

: trans-1-[6-(N,N-dimethylamino)hexylthio]-2-(dimethyloctylsilyl)-4-[6-(N,N-dimethylamino)hexanoxycarbonyl]-5-(octanoxycarbonyl)-1-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 24 h

2: 36 percent / 4-tert-butylcatechol / toluene / 24 h / 85 °C

With dmap; 4-tert-Butylcatechol; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Esterification / 2: Diels-Alder reaction;
DOI:10.1021/ja9940571