(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol

Base Information

• Chemical Name: (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol
• CAS No.: 1039740-26-5
• Molecular Formula: C₂₁H₃₂O₅
• Molecular Weight: 364.482

Synonyms:(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol

Chemical Property of (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol

Chemical Property:

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Technology Process of (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol

There total 1 articles about (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol (1039740-24-3) + p-methoxybenzyl chloride (824-94-2) → (1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol (1039740-26-5)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at -60 - 20 ℃; for 12h;

DOI:10.1021/jo800913x

Reference yield: 91.0%

(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexanol (1039740-26-5) + t-butyldimethylsiyl triflate (69739-34-0) → tert-butyl[(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexyloxy]dimethylsilane (1039740-28-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1021/jo800913x

upstream raw materials:

(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-(hydroxymethyl)-2-methyl-4-methylenecyclohexanol

p-methoxybenzyl chloride

Downstream raw materials:

tert-butyl[(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexyloxy]dimethylsilane

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